Details:

Personal Author:
Sloan, Catherine A.; Anulacion, Bernadita F.; Baugh, Keri A.; Bolton, Jennie L.; Boyd, Daryle; ... More +
Sloan, Catherine A.; Anulacion, Bernadita F.; Baugh, Keri A.; Bolton, Jennie L.; Boyd, Daryle; Boyer, Richard H.; Burrows, Douglas G.; Herman, David P.; Pearce, R. (Ronald); Ylitalo, Gina Maria; Less -
Corporate Authors:
Northwest Fisheries Science Center (U.S.); United States, National Oceanic and Atmospheric Administration;
Northwest Fisheries Science Center (U.S.); United States, National Oceanic and Atmospheric Administration; Less -
NOAA Program & Office:
NMFS (National Marine Fisheries Service); NWFSC (Northwest Fisheries Science Center);
NMFS (National Marine Fisheries Service); NWFSC (Northwest Fisheries Science Center); Less -
Description:
"This document describes the analytical methods developed and currently used by the Environmental Chemistry Program in the Environmental Conservation Division of the Northwest Fisheries Science Center for the analysis of sediment, tissue, and water samples for part-per-billion concentrations (nanograms per gram or nanograms per milliliter) of selected polycyclic aromatic hydrocarbons and persistent organic pollutants, plus selected alkanes in water samples as needed. Detailed descriptions are presented for sample extraction, cleanup by silica/alumina columns and by size-exclusion high-performance liquid chromatography, and analysis by gas chromatography/mass spectrometry, as well as the calculation of analyte concentrations and important quality assurance measurements. Detailed descriptions are also given for measuring lipid classes in tissues, determining the percent total extractable content of tissues, and determining the percent dry weight of tissues and sediments. Information pertaining to the necessary laboratory supplies and instruments is provided. The step-wise procedures are presented in a descriptive manner, which facilitates the use of this document by other laboratories"--Executive summary.
Content Notes:
Catherine A. Sloan, Bernadita F. Anulacion, Keri A. Baugh, Jennie L. Bolton, Daryle Boyd, Richard H. Boyer, Douglas G. Burrows, David P. Herman, Ronald W. Pearce, and Gina M. Ylitalo. Also available online in PDF format. Includes bibliographical references (page 61).
Keywords:
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Analysis
Contaminated Sediments
Environmental Sampling
Gas Chromatography
Marine Sediments
Mass Spectrometry
Measurement
Organic Water Pollutants
Pollution
Research
Water

Series:
NOAA technical memorandum NMFS-NWFSC ; 125;
Document Type:
Technical Memorandum;
Place as Subject:
United States;
Rights Information:
Public Domain
Compliance:
Library
Main Document Checksum:
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urn:sha256:e2251addf57c49dce8fd97f03a029c2f73f82f5b2f5ec23100a58262f05bd77a
File Type:

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